TA Instruments

AR1714-0001f

04/09/2012 17:27:27

Sample name	ASW 10 mm from base, 60 mm to top, disk 2 PMMA Br fouled
Sample notes	 
Experiment notes	Plastic parallel plate with adaptor supplied by Southampton Uni., on ETC rod with grub screws.

Distances fromlower surface of PP plate. Southampton container.
Operator	M Rides
Sample density	1.000 g/cm^3
Results file name	AR1714
Run number	1 
Results directory	D:\ARG2 rheometer\Test files\Southampton University P Stoodley May2012
Experiment was run on	04/09/2012 17:27:27

Procedure name	Flow procedure
Procedure notes	

Step name	Conditioning Step 1
Step notes	
Perform step	Yes
Initial temperature	22.4 C
Wait for correct temperature	Yes
Do set temperature	Yes
Wait for normal force	No
Perform pre-shear	No
Perform equilibration	Yes
Equilibration duration	0:01:00 hh:mm:ss
Wait for zero velocity	No
Control normal force	Uses current instrument settings
Purge gas only	No

Step name	Continuous ramp step 1
Step notes	
Perform step	Yes
Ramp type	Continuous ramp
Start controlled variable	velocity 3.000 rad/s
End controlled variable	velocity 300.0 rad/s
Duration	0:01:00 hh:mm:ss
Ramp mode	linear 
Delay time	0:00:01 hh:mm:ss
Temperature	22.4 C
Wait for temperature	No
Match duration and start value to previous step	No
Motor mode	auto 

Step name	Peak hold step
Step notes	
Perform step	Yes
Ramp type	Peak hold
Controlled variable	velocity 300.0 rad/s
Duration	0:00:30 hh:mm:ss
Delay time	0:00:01 hh:mm:ss
Temperature	22.4 C
Wait for temperature	No
Motor mode	auto 

Step name	Continuous ramp step 2
Step notes	
Perform step	Yes
Ramp type	Continuous ramp
Start controlled variable	velocity 300.0 rad/s
End controlled variable	velocity 3.000 rad/s
Duration	0:01:00 hh:mm:ss
Ramp mode	linear 
Delay time	0:00:01 hh:mm:ss
Temperature	22.4 C
Wait for temperature	No
Match duration and start value to previous step	No
Motor mode	auto 

Step name	Post-Experiment Step
Step notes	
Perform step	Yes
Do set temperature	Yes
Temperature	22.4 C
Set temperature system idle	No

Geometry name	25mm ETC plastic plate Southampton
Geometry notes	25 mm diameter parallel plastic plate with ETC rod
Geometry material	Other
Parallel plate diameter	25.00 mm
gap	10000 micro m
Gap offset	0 micro m
Geometry inertia	3.100 micro N.m.s^2
Geometry compliance	2.020E-3 rad/N.m
Gap temperature compensation	0 micro m/C
Gap temperature compensation enabled	No
Shear rate factor	1.250 
Shear stress factor	3.259E5 1/m^3
Measurement system factor	2.608E5 1/m^3
Fluid density factor	1.278E-10 m^5
Normal force factor	4074 1/m^2
Backoff distance	5000 micro m
Approximate sample volume	4.91 ml

Sample compression	linear 
Compression distance	1000.0 micro m
Compression velocity	50.0 micro m/s
Fine velocity	500.0 micro m/s
Coarse velocity	6000.0 micro m/s
Other velocity	6000.0 micro m/s
Current temperature system	Peltier plate
Temperature control	Enabled 
Purge gas only	No
Temperature calibration	Peltier plate - 0 micro m/C
	Water bath - 0 micro m/C
	Torsion oven - plate - 0 micro m/C
	Torsion oven - solid sample - 0 micro m/C
	Peltier concentric cylinders - 0 micro m/C
	None - 0 micro m/C
	Stress relaxation - 0 micro m/C
	Current temperature system - 0 micro m/C
Cooling water temperature	15.0 C
Cooling water range	6.0 C
Bearing friction correction	Yes
Bearing friction	0.262 micro N.m/(rad/s)
Bearing offset	0 micro N.m
Temperature system span and offset	Peltier plate - span 1.0000 , offset 0 C
	Water bath - span 1.0000 , offset 0 C
	Torsion oven - plate - span 1.0000 , offset 0 C
	Torsion oven - solid sample - span 1.0000 , offset 0 C
	Peltier concentric cylinders - span 1.0000 , offset 0 C
	None - span 1.0000 , offset 0 C
	Stress relaxation - span 1.0000 , offset 0 C
	Current temperature system - span 1.0000 , offset 0 C
Bearing mapping type	precision 
Number of mapping iterations	3
Instrument type (MType)	AR-G2
Firmware version	  8.29  27/10/09
Configuration version (CnfVer)	301
Parameter version (PrmVer)	301
PCB Number	*NOT_SET*
IP address	192.168.1.2
Software version	V5.8.0
Windows version	Windows XP 5.1 (Service Pack 2)
Instrument inertia	18.42 micro N.m.s^2
Auto increment run number	Yes
Prompt for file name at start of run	Yes
Auto save results file	Yes
Results file storage	Consecutive steps of same type to 1 file 
Temperature tolerance	0.2 C
Temperature duration	0:00:10 hh:mm:ss
Wait for temperature even if OK	Yes
Gap tolerance	4 micro m
Gap duration	0:00:02 hh:mm:ss
Override wait for gap	No
Velocity tolerance	0.1000 rad/s
Zero speed after pre-shear	Leave as is 
Zero normal force before run	No
Zero timer before run	Before pre-shear 
Non-equilibrium minimum velocity	1.000E-4 rad/s
Zero strain at the start of each flow step	Yes
Inertia correction	Yes
Collect negative shear rate data if stress is positive	Yes
Collect all points	No
Display flow point graph during run	Yes
Store flow point graph with results	Yes
Store images to the results for flow steps	Yes
Creep zero displacement	Yes
Store images to the results for creep steps	Yes
Standard creep image store frequency	10 s
Repeated creep image store frequency in repeats	10 
Display oscillation waveform graph during run	Yes
Store oscillation waveform graph with results	Yes
Display strain control tries during run	Yes
Store strain control tries with results	Yes
Store images to the results for oscillation steps	Yes
Stress relaxation zero displacement	Yes
Store images to the results for stress relaxation steps	Yes
Flow torque limit	10.00 micro N.m
Flow velocity limit	1.000E-3 rad/s
Oscillation torque limit	5.00 micro N.m
Oscillation displacement limit	1.00E-5 rad
Oscillation raw phase limit	170.0 degrees
Oscillation minimum normal force limit	0.1000 N
Oscillation maximum normal force limit	50.00 N
Flow velocity tolerance	1.00 %
Oscillation torque tolerance	1.00 %
Oscillation displacement tolerance	1.00 %
Oscillation velocity tolerance	1.00 %
Temperature tolerance	1.0 C

Continuous ramp step 1

shear stress	shear rate	viscosity	time	temperature	normal stress	displacement	gap	normal force	normal stress coefficient	strain	% strain	1/temperature	time	time global	time global	torque	velocity
Pa	1/s	Pa.s	s	C	Pa	rad	micro m	N	Pa.s^2			1/K	min	min	s	micro N.m	rad/s

-11.42	7.635	-1.496	0.99600	22.4	741.5	5.3993	10000	0.1820	12.72	6.7491	674.91	3.384E-3	0.0	1.0	60.996	-35.038	6.108
0.8363	12.28	0.06808	1.9960	22.4	746.5	13.2126	10000	0.1832	4.948	16.516	1651.6	3.384E-3	0.0	1.0	61.996	2.5656	9.826
1.700	19.34	0.08788	3.0080	22.4	737.4	26.8621	10000	0.1810	1.971	33.578	3357.8	3.384E-3	0.1	1.1	63.008	5.2149	15.47
2.316	23.02	0.1006	3.9960	22.4	741.5	41.2135	10000	0.1820	1.400	51.517	5151.7	3.383E-3	0.1	1.1	63.996	7.1061	18.41
3.634	30.82	0.1179	4.9960	22.4	742.3	67.4687	10000	0.1822	0.7817	84.336	8433.6	3.383E-3	0.1	1.1	64.996	11.150	24.65
5.663	39.46	0.1435	5.9960	22.4	743.2	106.6020	10000	0.1824	0.4772	133.25	13325	3.384E-3	0.1	1.1	65.996	17.374	31.57
6.329	42.52	0.1488	6.9960	22.4	735.7	126.5470	10000	0.1806	0.4069	158.18	15818	3.384E-3	0.1	1.1	66.996	19.417	34.02
8.105	49.11	0.1650	7.9960	22.4	722.5	165.3240	10000	0.1773	0.2995	206.66	20666	3.384E-3	0.1	1.1	67.996	24.867	39.29
10.74	57.53	0.1867	8.9960	22.4	738.2	223.2970	10000	0.1812	0.2231	279.12	27912	3.384E-3	0.1	1.1	68.996	32.950	46.02
12.64	63.68	0.1985	9.9960	22.4	726.6	275.9970	10000	0.1783	0.1792	345.00	34500	3.384E-3	0.2	1.2	69.996	38.779	50.94
14.71	69.62	0.2113	10.996	22.4	722.5	325.8080	10000	0.1773	0.1490	407.26	40726	3.383E-3	0.2	1.2	70.996	45.131	55.70
16.81	75.09	0.2239	11.996	22.4	729.9	376.9640	10000	0.1792	0.1294	471.21	47121	3.384E-3	0.2	1.2	71.996	51.579	60.07
18.85	80.49	0.2342	12.996	22.4	726.6	434.4790	10000	0.1783	0.1122	543.10	54310	3.384E-3	0.2	1.2	72.996	57.827	64.39
21.37	86.41	0.2473	13.996	22.4	711.7	498.5710	10000	0.1747	0.09531	623.21	62321	3.384E-3	0.2	1.2	73.996	65.551	69.13
24.95	94.58	0.2637	14.996	22.4	706.8	596.9720	10000	0.1735	0.07901	746.22	74622	3.383E-3	0.2	1.2	74.996	76.531	75.66
26.99	99.89	0.2702	15.996	22.4	718.4	663.9930	10000	0.1763	0.07199	829.99	82999	3.383E-3	0.3	1.3	75.996	82.796	79.91
29.64	105.6	0.2806	16.996	22.4	703.5	740.3770	10000	0.1727	0.06304	925.47	92547	3.383E-3	0.3	1.3	76.996	90.929	84.51
33.66	113.7	0.2960	17.996	22.4	695.2	854.8720	10000	0.1706	0.05377	1068.6	1.0686E5	3.384E-3	0.3	1.3	77.996	103.25	90.97
36.32	119.0	0.3053	18.996	22.4	695.2	937.2510	10000	0.1706	0.04911	1171.6	1.1716E5	3.383E-3	0.3	1.3	78.996	111.44	95.18
39.07	124.6	0.3135	19.996	22.4	688.6	1026.1899	10000	0.1690	0.04434	1282.7	1.2827E5	3.383E-3	0.3	1.3	79.996	119.85	99.70
42.02	130.0	0.3232	20.996	22.4	705.1	1115.0200	10000	0.1731	0.04171	1393.8	1.3938E5	3.383E-3	0.3	1.3	80.996	128.91	104.0
45.61	137.7	0.3312	21.992	22.4	666.3	1249.2900	10000	0.1635	0.03513	1561.6	1.5616E5	3.384E-3	0.4	1.4	81.992	139.92	110.2
48.90	143.1	0.3417	22.996	22.4	676.2	1349.5601	10000	0.1660	0.03301	1687.0	1.6870E5	3.383E-3	0.4	1.4	82.996	150.02	114.5
51.68	148.5	0.3480	23.996	22.4	682.8	1450.9800	10000	0.1676	0.03096	1813.7	1.8137E5	3.384E-3	0.4	1.4	83.996	158.55	118.8
55.96	156.2	0.3582	24.996	22.4	667.9	1604.3400	10000	0.1639	0.02737	2005.4	2.0054E5	3.383E-3	0.4	1.4	84.996	171.70	125.0
59.03	161.6	0.3653	25.996	22.4	677.0	1716.9301	10000	0.1662	0.02592	2146.2	2.1462E5	3.384E-3	0.4	1.4	85.996	181.11	129.3
62.64	167.0	0.3752	26.996	22.4	674.5	1888.7100	10000	0.1656	0.02419	2360.9	2.3609E5	3.383E-3	0.4	1.4	86.996	192.19	133.6
67.75	174.7	0.3878	27.996	22.4	676.2	2001.7900	10000	0.1660	0.02215	2502.2	2.5022E5	3.384E-3	0.5	1.5	87.996	207.84	139.8
70.65	179.8	0.3929	28.992	22.4	666.3	2121.9800	10000	0.1635	0.02061	2652.5	2.6525E5	3.384E-3	0.5	1.5	88.992	216.76	143.9
75.79	187.8	0.4036	29.996	22.4	659.7	2311.8101	10000	0.1619	0.01870	2889.8	2.8898E5	3.384E-3	0.5	1.5	89.996	232.51	150.2
79.44	192.9	0.4117	30.996	22.4	656.4	2440.7200	10000	0.1611	0.01763	3050.9	3.0509E5	3.384E-3	0.5	1.5	90.996	243.72	154.3
83.50	198.1	0.4216	31.996	22.4	652.2	2572.5801	10000	0.1601	0.01663	3215.7	3.2157E5	3.384E-3	0.5	1.5	91.996	256.16	158.4
88.79	206.0	0.4309	32.996	22.4	644.0	2780.6599	10000	0.1581	0.01517	3475.8	3.4758E5	3.384E-3	0.5	1.5	92.996	272.42	164.8
92.54	211.2	0.4382	33.996	22.4	634.9	2918.8799	10000	0.1558	0.01423	3648.6	3.6486E5	3.384E-3	0.6	1.6	93.996	283.91	169.0
96.68	218.8	0.4419	34.996	22.4	629.1	3134.4700	10000	0.1544	0.01314	3918.1	3.9181E5	3.384E-3	0.6	1.6	94.996	296.62	175.0
100.2	224.1	0.4470	35.996	22.4	626.6	3287.5000	10000	0.1538	0.01248	4109.4	4.1094E5	3.384E-3	0.6	1.6	95.996	307.34	179.3
104.1	229.3	0.4539	36.996	22.4	639.0	3437.8899	10000	0.1568	0.01216	4297.4	4.2974E5	3.384E-3	0.6	1.6	96.996	319.30	183.4
110.8	236.9	0.4678	38.000	22.4	622.5	3671.3799	10000	0.1528	0.01109	4589.2	4.5892E5	3.384E-3	0.6	1.6	98.000	339.99	189.5
115.3	242.2	0.4759	39.000	22.4	596.0	3835.2800	10000	0.1463	0.01016	4794.1	4.7941E5	3.384E-3	0.7	1.7	99.000	353.65	193.8
120.4	250.0	0.4818	39.996	22.4	615.0	4083.4500	10000	0.1510	9.844E-3	5104.3	5.1043E5	3.384E-3	0.7	1.7	99.996	369.51	200.0
124.6	255.0	0.4886	40.996	22.4	615.0	4244.7202	10000	0.1510	9.460E-3	5305.9	5.3059E5	3.383E-3	0.7	1.7	100.996	382.23	204.0
130.1	260.2	0.4999	41.996	22.4	598.5	4421.5098	10000	0.1469	8.841E-3	5526.9	5.5269E5	3.384E-3	0.7	1.7	101.996	399.01	208.2
136.1	268.0	0.5078	42.996	22.4	592.7	4688.4502	10000	0.1455	8.255E-3	5860.6	5.8606E5	3.384E-3	0.7	1.7	102.996	417.48	214.4
138.9	273.0	0.5089	43.996	22.4	586.9	4863.3101	10000	0.1441	7.874E-3	6079.1	6.0791E5	3.384E-3	0.7	1.7	103.996	426.22	218.4
148.2	280.7	0.5280	44.996	22.4	568.7	5141.0400	10000	0.1396	7.219E-3	6426.3	6.4263E5	3.383E-3	0.7	1.7	104.996	454.64	224.5
151.7	285.8	0.5307	45.996	22.4	600.2	5330.2798	10000	0.1473	7.345E-3	6662.9	6.6629E5	3.384E-3	0.8	1.8	105.996	465.39	228.7
156.2	290.9	0.5370	46.996	22.4	568.7	5519.6499	10000	0.1396	6.720E-3	6899.6	6.8996E5	3.384E-3	0.8	1.8	106.996	479.29	232.7
164.9	298.6	0.5521	47.996	22.4	564.6	5816.0098	10000	0.1386	6.332E-3	7270.0	7.2700E5	3.384E-3	0.8	1.8	107.996	505.82	238.9
170.3	303.8	0.5604	48.996	22.4	551.4	6017.9600	10000	0.1353	5.974E-3	7522.5	7.5225E5	3.383E-3	0.8	1.8	108.996	522.35	243.0
176.6	311.4	0.5672	49.996	22.4	556.3	6320.7700	10000	0.1365	5.737E-3	7901.0	7.9010E5	3.383E-3	0.8	1.8	109.996	541.94	249.1
181.6	316.5	0.5739	50.996	22.4	569.6	6528.7998	10000	0.1398	5.687E-3	8161.0	8.1610E5	3.383E-3	0.8	1.8	110.996	557.15	253.2
189.1	324.2	0.5832	51.996	22.4	529.9	6853.2598	10000	0.1301	5.040E-3	8566.6	8.5666E5	3.383E-3	0.9	1.9	111.996	580.16	259.4
194.4	329.3	0.5904	52.996	22.4	529.1	7064.8901	10000	0.1299	4.879E-3	8831.1	8.8311E5	3.383E-3	0.9	1.9	112.996	596.47	263.4
198.7	334.3	0.5944	53.996	22.4	512.5	7283.2500	10000	0.1258	4.586E-3	9104.1	9.1041E5	3.383E-3	0.9	1.9	113.996	609.63	267.4
208.3	342.0	0.6091	54.996	22.4	477.0	7619.8398	10000	0.1171	4.078E-3	9524.8	9.5248E5	3.384E-3	0.9	1.9	114.996	639.16	273.6
213.8	347.1	0.6158	55.996	22.4	478.6	7846.7300	10000	0.1175	3.973E-3	9808.4	9.8084E5	3.383E-3	0.9	1.9	115.996	655.80	277.7
220.1	354.7	0.6205	56.996	22.4	460.4	8193.5703	10000	0.1130	3.660E-3	10242	1.0242E6	3.383E-3	0.9	1.9	116.996	675.16	283.7
223.6	359.9	0.6214	57.996	22.4	449.7	8433.0400	10000	0.1104	3.472E-3	10541	1.0541E6	3.383E-3	1.0	2.0	117.996	686.02	287.9
232.3	367.5	0.6321	59.000	22.4	486.1	8793.7305	10000	0.1193	3.599E-3	10992	1.0992E6	3.384E-3	1.0	2.0	119.000	712.68	294.0
237.8	372.5	0.6382	59.996	22.4	467.1	9031.8701	10000	0.1146	3.366E-3	11290	1.1290E6	3.384E-3	1.0	2.0	119.996	729.44	298.0

Peak hold step

shear stress	shear rate	viscosity	time	temperature	normal stress	displacement	gap	normal force	normal stress coefficient	strain	% strain	1/temperature	time	time global	time global	torque	velocity
Pa	1/s	Pa.s	s	C	Pa	rad	micro m	N	Pa.s^2			1/K	min	min	s	micro N.m	rad/s

240.5	375.0	0.6414	1.0000	22.4	481.1	325.9570	10000	0.1181	3.421E-3	407.45	40745	3.384E-3	0.0	2.0	122.000	737.91	300.0
240.5	375.0	0.6414	2.0160	22.4	426.6	574.8860	10000	0.1047	3.033E-3	718.61	71861	3.384E-3	0.0	2.1	123.016	737.95	300.0
241.2	375.0	0.6432	3.0200	22.4	456.3	826.3680	10000	0.1120	3.245E-3	1033.0	1.0330E5	3.384E-3	0.1	2.1	124.020	740.02	300.0
245.5	375.0	0.6547	4.0000	22.4	459.6	1205.0300	10000	0.1128	3.269E-3	1506.3	1.5063E5	3.384E-3	0.1	2.1	125.000	753.15	300.0
243.4	375.0	0.6492	5.0160	22.4	428.2	1455.4900	10000	0.1051	3.045E-3	1819.4	1.8194E5	3.384E-3	0.1	2.1	126.016	746.89	300.0
243.5	375.0	0.6495	6.0000	22.4	442.3	1831.7200	10000	0.1085	3.145E-3	2289.7	2.2897E5	3.384E-3	0.1	2.1	127.000	747.20	300.0
242.7	375.0	0.6473	7.0000	22.4	501.8	2084.3501	10000	0.1232	3.568E-3	2605.4	2.6054E5	3.384E-3	0.1	2.1	128.000	744.73	300.0
240.1	375.0	0.6403	8.0200	22.4	477.8	2336.2700	10000	0.1173	3.398E-3	2920.3	2.9203E5	3.384E-3	0.1	2.2	129.020	736.73	300.0
241.7	375.0	0.6444	9.0160	22.4	462.9	2712.4800	10000	0.1136	3.292E-3	3390.6	3.3906E5	3.384E-3	0.2	2.2	130.016	741.40	300.0
238.1	375.0	0.6348	9.9960	22.4	473.7	2962.6899	10000	0.1163	3.368E-3	3703.4	3.7034E5	3.383E-3	0.2	2.2	130.996	730.35	300.0
237.5	375.0	0.6334	11.000	22.4	466.2	3213.8501	10000	0.1144	3.315E-3	4017.3	4.0173E5	3.383E-3	0.2	2.2	132.000	728.76	300.0
241.7	375.0	0.6445	12.000	22.4	439.8	3591.9600	10000	0.1079	3.127E-3	4490.0	4.4900E5	3.384E-3	0.2	2.2	133.000	741.44	300.0
243.6	375.0	0.6498	13.020	22.4	461.3	3842.3501	10000	0.1132	3.281E-3	4802.9	4.8029E5	3.384E-3	0.2	2.2	134.020	747.50	300.0
243.3	375.0	0.6487	14.000	22.4	455.5	4225.6699	10000	0.1118	3.239E-3	5282.1	5.2821E5	3.383E-3	0.2	2.3	135.000	746.30	300.0
240.8	375.0	0.6422	14.992	22.4	449.7	4470.6899	10000	0.1104	3.198E-3	5588.4	5.5884E5	3.384E-3	0.2	2.3	135.992	738.82	300.0
241.9	375.0	0.6452	15.996	22.4	443.1	4722.0601	10000	0.1088	3.151E-3	5902.6	5.9026E5	3.384E-3	0.3	2.3	136.996	742.26	300.0
241.7	375.0	0.6444	17.000	22.4	453.0	5100.4399	10000	0.1112	3.221E-3	6375.6	6.3756E5	3.384E-3	0.3	2.3	138.000	741.43	300.0
238.1	375.0	0.6350	17.996	22.4	469.5	5350.2100	10000	0.1152	3.339E-3	6687.8	6.6878E5	3.384E-3	0.3	2.3	138.996	730.62	300.0
241.3	375.0	0.6436	19.000	22.4	453.8	5727.3398	10000	0.1114	3.227E-3	7159.2	7.1592E5	3.384E-3	0.3	2.3	140.000	740.44	300.0
239.9	375.0	0.6397	19.992	22.4	477.0	5978.6201	10000	0.1171	3.392E-3	7473.3	7.4733E5	3.384E-3	0.3	2.3	140.992	735.93	300.0
239.6	375.0	0.6389	21.000	22.4	533.2	6231.0498	10000	0.1309	3.791E-3	7788.8	7.7888E5	3.383E-3	0.4	2.4	142.000	735.11	300.0
242.1	375.0	0.6455	22.012	22.4	454.7	6614.2300	10000	0.1116	3.233E-3	8267.8	8.2678E5	3.384E-3	0.4	2.4	143.012	742.69	300.0
241.3	375.0	0.6434	23.008	22.4	474.5	6859.4502	10000	0.1165	3.374E-3	8574.3	8.5743E5	3.383E-3	0.4	2.4	144.008	740.21	300.0
243.6	375.0	0.6495	24.000	22.4	434.8	7236.7798	10000	0.1067	3.092E-3	9046.0	9.0460E5	3.383E-3	0.4	2.4	145.000	747.23	300.0
241.1	375.0	0.6428	25.012	22.4	436.5	7486.6699	10000	0.1071	3.104E-3	9358.3	9.3583E5	3.384E-3	0.4	2.4	146.012	739.54	300.0
242.6	375.0	0.6470	25.992	22.4	444.7	7739.1499	10000	0.1092	3.163E-3	9673.9	9.6739E5	3.383E-3	0.4	2.4	146.992	744.36	300.0
244.7	375.0	0.6525	27.000	22.4	429.0	8116.1201	10000	0.1053	3.051E-3	10145	1.0145E6	3.383E-3	0.5	2.5	148.000	750.72	300.0
241.6	375.0	0.6441	28.000	22.4	438.1	8367.4697	10000	0.1075	3.115E-3	10459	1.0459E6	3.384E-3	0.5	2.5	149.000	741.07	300.0
243.7	375.0	0.6499	28.996	22.4	485.2	8621.7402	10000	0.1191	3.451E-3	10777	1.0777E6	3.384E-3	0.5	2.5	149.996	747.72	300.0
241.7	375.0	0.6445	30.012	22.4	485.2	8997.6201	10000	0.1191	3.451E-3	11247	1.1247E6	3.384E-3	0.5	2.5	151.012	741.48	300.0

Continuous ramp step 2

shear stress	shear rate	viscosity	time	temperature	normal stress	displacement	gap	normal force	normal stress coefficient	strain	% strain	1/temperature	time	time global	time global	torque	velocity
Pa	1/s	Pa.s	s	C	Pa	rad	micro m	N	Pa.s^2			1/K	min	min	s	micro N.m	rad/s

239.4	372.0	0.6435	0.99200	22.4	435.6	230.5340	10000	0.1069	3.148E-3	288.17	28817	3.383E-3	0.0	2.5	151.992	734.37	297.6
228.4	364.4	0.6266	1.9920	22.4	478.6	586.2780	10000	0.1175	3.604E-3	732.85	73285	3.383E-3	0.0	2.5	152.992	700.57	291.5
223.9	359.3	0.6230	3.0080	22.4	471.2	824.1600	10000	0.1156	3.649E-3	1030.2	1.0302E5	3.383E-3	0.1	2.6	154.008	686.82	287.5
216.9	351.6	0.6167	4.0040	22.4	480.3	1174.7700	10000	0.1179	3.885E-3	1468.5	1.4685E5	3.383E-3	0.1	2.6	155.004	665.29	281.3
212.8	346.6	0.6139	4.9920	22.4	519.1	1401.5900	10000	0.1274	4.320E-3	1752.0	1.7520E5	3.384E-3	0.1	2.6	155.992	652.82	277.3
204.3	341.6	0.5980	5.9920	22.4	513.3	1625.6300	10000	0.1260	4.400E-3	2032.0	2.0320E5	3.384E-3	0.1	2.6	156.992	626.72	273.3
195.5	333.8	0.5856	6.9920	22.4	510.0	1964.5500	10000	0.1252	4.576E-3	2455.7	2.4557E5	3.384E-3	0.1	2.6	157.992	599.80	267.1
192.1	328.8	0.5844	8.0280	22.4	497.6	2176.5901	10000	0.1221	4.603E-3	2720.7	2.7207E5	3.384E-3	0.1	2.7	159.028	589.45	263.0
185.3	321.2	0.5768	9.0080	22.4	524.9	2495.8401	10000	0.1288	5.088E-3	3119.8	3.1198E5	3.384E-3	0.2	2.7	160.008	568.36	257.0
180.8	316.0	0.5720	9.9920	22.4	543.1	2709.5100	10000	0.1333	5.438E-3	3386.9	3.3869E5	3.383E-3	0.2	2.7	160.992	554.56	252.8
174.3	308.3	0.5653	11.008	22.4	532.4	3015.2400	10000	0.1307	5.600E-3	3769.1	3.7691E5	3.384E-3	0.2	2.7	162.008	534.76	246.7
168.7	303.3	0.5563	12.008	22.4	523.3	3218.6299	10000	0.1284	5.689E-3	4023.3	4.0233E5	3.384E-3	0.2	2.7	163.008	517.64	242.6
161.8	298.1	0.5428	12.992	22.4	540.6	3416.0000	10000	0.1327	6.083E-3	4270.0	4.2700E5	3.384E-3	0.2	2.7	163.992	496.47	238.5
154.0	290.5	0.5301	13.992	22.4	571.2	3704.9900	10000	0.1402	6.769E-3	4631.2	4.6312E5	3.384E-3	0.2	2.7	164.992	472.43	232.4
149.4	285.4	0.5234	15.008	22.4	557.2	3891.4199	10000	0.1367	6.838E-3	4864.3	4.8643E5	3.384E-3	0.3	2.8	166.008	458.36	228.4
142.2	277.7	0.5121	15.992	22.4	604.3	4172.8999	10000	0.1483	7.835E-3	5216.1	5.2161E5	3.384E-3	0.3	2.8	166.992	436.34	222.2
139.2	272.5	0.5106	16.992	22.4	577.8	4356.0000	10000	0.1418	7.780E-3	5445.0	5.4450E5	3.384E-3	0.3	2.8	167.992	426.94	218.0
132.6	264.9	0.5005	17.992	22.4	591.9	4618.4302	10000	0.1453	8.432E-3	5773.0	5.7730E5	3.384E-3	0.3	2.8	168.992	406.85	211.9
128.6	259.8	0.4951	18.992	22.4	582.0	4792.8799	10000	0.1428	8.623E-3	5991.1	5.9911E5	3.384E-3	0.3	2.8	169.992	394.58	207.8
126.5	254.5	0.4969	19.988	22.4	591.1	4967.3198	10000	0.1451	9.124E-3	6209.2	6.2092E5	3.384E-3	0.3	2.8	170.988	388.02	203.6
119.5	246.9	0.4838	21.008	22.4	588.6	5211.3198	10000	0.1445	9.655E-3	6514.2	6.5142E5	3.384E-3	0.4	2.9	172.008	366.50	197.5
113.8	241.8	0.4709	21.992	22.4	613.4	5376.4800	10000	0.1505	0.01049	6720.6	6.7206E5	3.384E-3	0.4	2.9	172.992	349.27	193.4
109.7	233.9	0.4689	23.012	22.4	592.7	5611.4302	10000	0.1455	0.01083	7014.3	7.0143E5	3.384E-3	0.4	2.9	174.012	336.52	187.1
105.6	228.9	0.4612	23.992	22.4	620.8	5761.2798	10000	0.1524	0.01185	7201.6	7.2016E5	3.383E-3	0.4	2.9	174.992	323.88	183.1
100.8	223.8	0.4504	24.992	22.4	635.7	5912.1899	10000	0.1560	0.01269	7390.2	7.3902E5	3.384E-3	0.4	2.9	175.992	309.20	179.0
93.94	215.9	0.4352	25.992	22.4	624.1	6137.8101	10000	0.1532	0.01339	7672.3	7.6723E5	3.384E-3	0.4	2.9	176.992	288.20	172.7
90.27	210.8	0.4283	27.008	22.4	633.2	6273.6602	10000	0.1554	0.01425	7842.1	7.8421E5	3.383E-3	0.5	3.0	178.008	276.95	168.6
87.23	203.1	0.4296	27.996	22.4	634.0	6481.7002	10000	0.1556	0.01538	8102.1	8.1021E5	3.383E-3	0.5	3.0	178.996	267.62	162.4
82.36	197.8	0.4165	29.008	22.4	642.3	6617.2900	10000	0.1576	0.01642	8271.6	8.2716E5	3.383E-3	0.5	3.0	180.008	252.68	158.2
78.79	192.7	0.4089	30.008	22.4	645.6	6742.8198	10000	0.1585	0.01739	8428.5	8.4285E5	3.383E-3	0.5	3.0	181.008	241.72	154.1
73.35	185.0	0.3964	30.992	22.4	651.4	6929.6099	10000	0.1599	0.01903	8662.0	8.6620E5	3.383E-3	0.5	3.0	181.992	225.03	148.0
70.05	179.7	0.3898	32.008	22.4	667.1	7054.8999	10000	0.1637	0.02065	8818.6	8.8186E5	3.384E-3	0.5	3.1	183.008	214.90	143.8
66.32	174.4	0.3803	33.008	22.4	674.5	7230.0601	10000	0.1656	0.02218	9037.6	9.0376E5	3.384E-3	0.6	3.1	184.008	203.47	139.5
60.84	166.8	0.3648	33.992	22.4	664.6	7341.3198	10000	0.1631	0.02390	9176.7	9.1767E5	3.384E-3	0.6	3.1	184.992	186.66	133.4
58.13	161.5	0.3600	34.996	22.4	674.5	7454.0601	10000	0.1656	0.02587	9317.6	9.3176E5	3.383E-3	0.6	3.1	185.996	178.35	129.2
55.11	156.0	0.3533	35.996	22.4	669.6	7616.6299	10000	0.1643	0.02751	9520.8	9.5208E5	3.384E-3	0.6	3.1	186.996	169.08	124.8
49.80	148.2	0.3359	37.008	22.4	688.6	7715.3198	10000	0.1690	0.03134	9644.2	9.6442E5	3.383E-3	0.6	3.1	188.008	152.78	118.6
47.09	142.9	0.3295	38.008	22.4	686.1	7815.4800	10000	0.1684	0.03359	9769.4	9.7694E5	3.384E-3	0.6	3.2	189.008	144.48	114.3
43.71	137.4	0.3181	39.008	22.4	695.2	7916.3101	10000	0.1706	0.03681	9895.4	9.8954E5	3.384E-3	0.7	3.2	190.008	134.11	109.9
40.09	129.7	0.3091	40.008	22.4	698.5	8045.3999	10000	0.1714	0.04154	10057	1.0057E6	3.384E-3	0.7	3.2	191.008	122.99	103.7
37.36	124.4	0.3004	40.996	22.4	696.0	8132.4902	10000	0.1708	0.04499	10166	1.0166E6	3.384E-3	0.7	3.2	191.996	114.63	99.50
35.00	118.8	0.2945	41.992	22.4	702.7	8257.1201	10000	0.1725	0.04976	10321	1.0321E6	3.384E-3	0.7	3.2	192.992	107.39	95.07
31.52	111.1	0.2837	43.008	22.4	719.2	8331.9199	10000	0.1765	0.05826	10415	1.0415E6	3.384E-3	0.7	3.2	194.008	96.696	88.88
28.75	105.8	0.2718	43.992	22.4	701.8	8405.8604	10000	0.1723	0.06272	10507	1.0507E6	3.384E-3	0.7	3.2	194.992	88.215	84.63
26.19	100.2	0.2614	44.996	22.4	729.9	8480.2598	10000	0.1792	0.07271	10600	1.0600E6	3.383E-3	0.7	3.3	195.996	80.349	80.15
22.82	91.96	0.2481	46.008	22.4	707.6	8579.6504	10000	0.1737	0.08368	10725	1.0725E6	3.383E-3	0.8	3.3	197.008	69.998	73.57
20.58	86.58	0.2377	46.992	22.4	716.7	8641.4297	10000	0.1759	0.09561	10802	1.0802E6	3.383E-3	0.8	3.3	197.992	63.144	69.26
18.60	80.86	0.2300	47.992	22.4	721.7	8703.2305	10000	0.1771	0.1104	10879	1.0879E6	3.384E-3	0.8	3.3	198.992	57.055	64.69
16.14	75.04	0.2151	49.008	22.4	724.1	8758.7598	10000	0.1777	0.1286	10948	1.0948E6	3.383E-3	0.8	3.3	200.008	49.531	60.04
14.31	69.76	0.2051	49.992	22.4	724.1	8808.4502	10000	0.1777	0.1488	11011	1.1011E6	3.384E-3	0.8	3.3	200.992	43.907	55.81
11.31	61.02	0.1853	51.016	22.4	729.9	8882.0801	10000	0.1792	0.1961	11103	1.1103E6	3.384E-3	0.9	3.4	202.016	34.691	48.81
9.659	54.88	0.1760	52.020	22.4	729.9	8924.9502	10000	0.1792	0.2424	11156	1.1156E6	3.384E-3	0.9	3.4	203.020	29.634	43.90
8.081	49.41	0.1635	53.008	22.4	733.2	8961.5801	10000	0.1800	0.3003	11202	1.1202E6	3.383E-3	0.9	3.4	204.008	24.793	39.53
6.522	43.31	0.1506	53.996	22.4	733.2	8998.4297	10000	0.1800	0.3910	11248	1.1248E6	3.384E-3	0.9	3.4	204.996	20.009	34.65
4.954	36.89	0.1343	54.992	22.4	731.6	9028.2900	10000	0.1796	0.5375	11285	1.1285E6	3.384E-3	0.9	3.4	205.992	15.198	29.51
3.689	31.40	0.1175	56.008	22.4	725.0	9052.4404	10000	0.1779	0.7353	11316	1.1316E6	3.383E-3	0.9	3.5	207.008	11.317	25.12
2.526	24.83	0.1018	57.012	22.4	749.8	9076.0498	10000	0.1840	1.216	11345	1.1345E6	3.384E-3	1.0	3.5	208.012	7.7511	19.86
1.400	17.45	0.08023	58.012	22.4	734.9	9093.6602	10000	0.1804	2.413	11367	1.1367E6	3.384E-3	1.0	3.5	209.012	4.2955	13.96
1.070	14.62	0.07322	59.012	22.4	744.8	9099.1504	10000	0.1828	3.487	11374	1.1374E6	3.384E-3	1.0	3.5	210.012	3.2833	11.69
0.3823	8.019	0.04768	60.016	22.4	734.9	9107.2500	10000	0.1804	11.43	11384	1.1384E6	3.384E-3	1.0	3.5	211.016	1.1730	6.415

